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Flow-based system for the determination of titratable acidity in wines

dc.contributor.authorVidigal, Susana S. M. P.
dc.contributor.authorRamos, Ana T. C.
dc.contributor.authorRangel, António O. S. S.
dc.date.accessioned2016-06-28T15:36:56Z
dc.date.available2016-06-28T15:36:56Z
dc.date.issued2016
dc.description.abstractA flow injection analysis system with a spectrophotometric detection was arranged in order to develop a simple and fast methodology for the quantification of titratable acidity in different types of wines. In the proposed system, a precise volume of sample is injected in the carrier stream, composed by a mixture of OH− solution with the pH indicator, bromothymol blue (BTB). Consequently, a change on the colour of the carrier solution is achieved and quantified by spectrophotometry. Therefore, it was possible to establish a linear range up to 0.16 g/L expressed as tartaric acid, with a limit of detection and quantification of 0.01 and 0.05 g/L, respectively. The proposed work has a low sample and reagents consumption, only 96 μg of BTB, 336 mmol de OH− and 50 μL of sample were needed per assay. At the same time, a high determination rate was achieved, 75 determinations per hour. The developed methodology was applied on the quantification of total acidity in red and white table wine and port wine samples.pt_PT
dc.identifier.citationVIDIGAL, SUSANA S. M. P.; RAMOS, Ana T. C.; RANGEL, António O. S. S. - Flow-Based System for the Determination of Titratable Acidity in Wines. Food Analytical Methods. (2016) ISSN: 1936-9751. Vol. 9, nº 8, p.2241–2245pt_PT
dc.identifier.doi10.1007/s12161-016-0408-7pt_PT
dc.identifier.eid84955275540
dc.identifier.urihttp://hdl.handle.net/10400.14/20321
dc.identifier.wos000378902200012
dc.language.isoengpt_PT
dc.peerreviewedyespt_PT
dc.publisherSpringerpt_PT
dc.subjectBromothymol bluept_PT
dc.subjectFlow-injection systempt_PT
dc.subjectSpectrophotometrypt_PT
dc.subjectTitratable aciditypt_PT
dc.subjectTable and port winept_PT
dc.titleFlow-based system for the determination of titratable acidity in winespt_PT
dc.typejournal article
dspace.entity.typePublication
oaire.awardURIinfo:eu-repo/grantAgreement/FCT/SFRH/SFRH%2FBPD%2F78705%2F2011/PT
oaire.awardURIinfo:eu-repo/grantAgreement/FCT/3599-PPCDT/PEst-OE%2FEQB%2FLA0016%2F2013/PT
oaire.citation.conferencePlaceUnited Statespt_PT
oaire.citation.endPage2245
oaire.citation.issue8
oaire.citation.startPage2241
oaire.citation.volume9
oaire.fundingStreamSFRH
oaire.fundingStream3599-PPCDT
person.familyNameVidigal
person.familyNameSantos Silva Rangel
person.givenNameSusana
person.givenNameAntónio Osmaro
person.identifier.ciencia-id2919-B77C-11C0
person.identifier.ciencia-idD61D-7CFB-178A
person.identifier.orcid0000-0002-0213-063X
person.identifier.orcid0000-0002-6486-8947
person.identifier.ridM-4661-2013
person.identifier.scopus-author-id11739488200
person.identifier.scopus-author-id7004827387
project.funder.identifierhttp://doi.org/10.13039/501100001871
project.funder.identifierhttp://doi.org/10.13039/501100001871
project.funder.nameFundação para a Ciência e a Tecnologia
project.funder.nameFundação para a Ciência e a Tecnologia
rcaap.rightsrestrictedAccesspt_PT
rcaap.typearticlept_PT
relation.isAuthorOfPublication59453cc2-ee50-4a1d-bbfc-924ca6417004
relation.isAuthorOfPublication467be022-fd9c-4549-aa48-48ebcc1098eb
relation.isAuthorOfPublication.latestForDiscovery467be022-fd9c-4549-aa48-48ebcc1098eb
relation.isProjectOfPublication6f2f1bdc-134c-49e2-bdc8-b249ab6090b7
relation.isProjectOfPublication76842dfa-b675-443a-843b-f9555a0a9199
relation.isProjectOfPublication.latestForDiscovery76842dfa-b675-443a-843b-f9555a0a9199

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