Repository logo
 
No Thumbnail Available
Publication

Sequential determination of titratable acidity and tartaric acid in wines by flow injection spectrophotometry

Use this identifier to reference this record.
Name:Description:Size:Format: 
a707477h.pdf64.97 KBAdobe PDF Download

Advisor(s)

Abstract(s)

A flow injection manifold is proposed for the sequential determination of titratable (total) acidity based on a pseudotitration and of tartaric acid based on the formation of a coloured vanadate complex. The method involves in-line dialysis prior to injection to avoid interference from the sample background absorption in the spectrophotometric detection. The changes in the colour of both reactions were monitored using two flow cells aligned in the optical path of a single spectrophotometer. Wine samples were analysed without any sample pre-treatment; table wines in the range 1–10 g l21 (total acidity) and 0.5–4 g l21 (tartaric acid) and port wines in the range 1–8 g l21 (total acidity) and 0.5–5 g l21 (tartaric acid). Sixteen samples can be measured per hour, and the results were comparable to those obtained by reference procedures for both determinations. RSDs (n = 10) generally lower than 3% were obtained

Description

Keywords

Flow injection Total acidity Tartaric acid Wine

Citation

RANGEL, António O.S.S.; TÓTH, Ildikó V. - Sequential determination of titratable acidity and tartaric acid in wines by flow injection spectrophotometry. Analyst. ISSN 0003-2654. Vol. 123 (1998), p. 661–664

Research Projects

Organizational Units

Journal Issue

Publisher

Royal Society of Chemistry

CC License

Altmetrics