Utilize este identificador para referenciar este registo: http://hdl.handle.net/10400.14/16576
Título: A flow injection system coupled to a micro-guard cartridge for monitoring a vinification process
Autor: Vidigal, Susana
Rangel, António O. S.S.
Palavras-chave: Ethanol
Sugars
Port wine
Synthetic grape juice
automation
Data: 2014
Citação: VIDIGAL, Susana ; RANGEL, António O. S. S. - A flow injection system coupled to a micro-guard cartridge for monitoring a vinification process. Analytical Sciences. ISSN 0910-6340. Vol. 30 (2014), p. 1057-1062
Resumo: The present paper describes a flow-injection system coupled to a Micro-Guard cartridge and a miniaturized optical CCD detection system used to monitor the sugars (glucose/fructose) and ethanol content during alcoholic fermentation. The carrier stream (mobile phase) is composed of an aqueous sulfuric acid solution. The flow parameters were studied in order to obtain a good resolution and a wide dynamic concentration range, with a good repeatability. The relative standard deviation (RSD) obtained was inferior to 4%, for n = 3. It was possible to achieve a linear range of up to 12 g L(-1) of sugars and up to 2% (v/v) of ethanol with a detection limit of 2.3 g L(-1) and 0.4% (v/v), for sugars and ethanol concentrations, respectively. The proposed system was successfully applied to monitor a vinification process by the quantification of sugars and ethanol, and also in some finished port wines.
Peer review: yes
URI: http://hdl.handle.net/10400.14/16576
Versão do Editor: https://www.jstage.jst.go.jp/article/analsci/30/11/30_1057/_article
Aparece nas colecções:CBQF - Artigos em revistas internacionais com Arbitragem / Papers in international journals with Peer-review

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